Property |
Specification |
Test Method |
Appearance |
White crystals or granules |
Visual |
Assay (as C₆H₈O₇·H₂O) |
Typically 99.0% – 100.5% (anhydrous) or 99.5% – 101.0% (monohydrate) |
Titrimetry |
Water Content |
<= 0.5% (anhydrous) or ~8.0% (monohydrate) |
Karl Fischer Titration |
pH (of a 10% solution) |
3.0 – 3.5 |
Potentiometr |
Loss on Drying |
<= 0.1% |
Gravimetry |
Sulfate (as SO₄) |
<= 0.015% |
Ion Chromatography |
Chloride (as Cl) |
<= 0.001% |
Ion Chromatography |
Insoluble Matter |
<= 0.005% |
Gravimetry |
Oxalic Acid |
<= 0.036% |
Titrimetry |
Heavy Metals (as Pb) |
<= 1 ppm |
Atomic Absorption Spectroscopy (AAS) |
Arsenic (as As) |
<= 1 ppm (may not be included in all COA reports) |
Inductively Coupled Plasma Mass Spectrometry (ICP-MS) |